HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 70515097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | ethyl N-(2-cyano-3-ethoxyacryloyl)carbamate | HCID 230015 | — |
| Product | HCID 70515097 | HCID 70515097 | — |
Reaction Steps
Following the procedure of Example 1, α-cyano-β-ethoxy-N-ethoxycarbonylacrylamide is reacted with phenylhydrazine to give α-cyano-β-phenylhydrazino-N-ethoxycarbonylacrylamide, which in turn is cyclized by heating in tetralin, yielding 5-cyano-1-anilino-2,4-pyrimidinedione. The foregoing compound has been reported by G. Shaw, J. Chem. Soc., 1955, 1834-1840.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04411839 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-89e70e89171b4d689a3b83b564732d0b |
| Source note | uspto-grants-1983_10 |