HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13326257, compound → HCID 13326258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13326257 | HCID 13326257 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 13326258 | HCID 13326258 | — |
Reaction Steps
5-Carbethoxy-1-(2,4,6-trichloroanilino)-2,4-pyrimidinedione is dissolved in a hot mixture of concentrated HCl and glacial acetic acid (1:1) and is refluxed for 10 hours. The reaction mixture is cooled to RT and filtered, giving 5-carboxy-1-(2,4,6-trichloroanilino)-2,4-pyrimidinedione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04411839 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-51699b6932864830891acb5575650d49 |
| Source note | uspto-grants-1983_10 |