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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 648175Generated: October 30, 2026

ethanesulfenyl chloride → HCID 13326281, compound

https://huagongshe.com/reaction/648175

Reaction equation

Participants

RoleNameHCIDCharge
Reactantethanesulfenyl chlorideHCID 12275523—
ReactantHCID 20459817HCID 20459817—
SolventDichloromethaneHCID 6344—
SolventSodium HydroxideHCID 14798—
ProductHCID 13326281HCID 13326281—
ProductHCID 53938821HCID 53938821—

Reaction Steps

In the same manner as above, 6-cyano-1-(2,4,6-trichloroanilino)-2,4-pyrimidinedione in aqueous sodium hydroxide is reacted with ethylsulfenyl chloride in methylene chloride, followed by chromatography yields the compounds 6-cyano-3-ethylthio-(2,4,6-trichloroanilino)-2,4-pyrimidinedione and 6-cyano-1-(N-ethylthio-2,4,6-trichloroanilino)-2,4-pyrimidinedione.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04411839
Source datasetuspto-grants-1983_10
ORD IDord-0da385d837e3445196fa49d444c749c8
Source noteuspto-grants-1983_10