Sodium Hydroxide → Sodium 4-(11-hydroxyundecylamino)benzoate

HRID 648310Notes

Reaction equation

HRID 648310 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][NH:13][C:14]1[CH:22]=[CH:21][C:17]([C:18]([OH:20])=[O:19])=[CH:16][CH:15]=1.[OH-].[Na+:24]>C(O)C.O>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][NH:13][C:14]1[CH:15]=[CH:16][C:17]([C:18]([O-:20])=[O:19])=[CH:21][CH:22]=1.[Na+:24]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 204825254-(11-Hydroxyundecylamino)benzoic acid

Product 1

HCID 23720900Sodium 4-(11-hydroxyundecylamino)benzoate

Reagents, catalysts & solvents 1

HCID 19096565Water ethanolSolvent

Procedure

A mixture of 3.62 g. of 4-(11-hydroxyundecylamino)benzoic acid and 25 ml. of ethanol-water (9:1) containing 400 mg. of sodium hydroxide is stirred for 4 hours. The mixture is filtered and the solid washed with ethanol-water and dried in vacuo to yield sodium 4-(11-hydroxyundecylamino)benzoate as a white, amorphous solid.

Workup

  1. additionA mixture of 3.62 g
  2. filtrationThe mixture is filtered
  3. washthe solid washed with ethanol-water
  4. customdried in vacuo

Sources & evidence

ORD record
ord-2c463f9e249b4dc39b907dcd59908788
Source dataset
uspto-grants-1983_10
Patent number
US04411903

Reaction notes

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