HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 20482586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 20482486 | HCID 20482486 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20482586 | HCID 20482586 | — |
Reaction Steps
A solution of 10 g. of ethyl 4-(6-hydroxyhexadecylamino)benzoate and 2.4 ml. of pyridine in 50 ml. of chloroform is treated with 2.0 ml. of thionyl chloride, stirred under reflux for 1 hour, washed with 1 N hydrochloric acid and saturated aqueous sodium bicarbonate, dried over magnesium sulfate, and evaporated. The residue is crystallized from aqueous ethanol to yield the product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04411903 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-c943a0ffe10b452fa4dc77fb38a248b3 |
| Source note | uspto-grants-1983_10 |