HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[N-benzyloxycarbonyl-L-prolyl]morpholine → HCID 7175777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[N-benzyloxycarbonyl-L-prolyl]morpholine | HCID 13564348 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 7175777 | HCID 7175777 | 98.7% |
Reaction Steps
In 100 ml of ethanol was suspended 4.9 g of compound (83) and after adding thereto 250 mg of 10% palladium carbon, the mixture was stirred for 4 hours in a hydrogen stream. After filtering off 10% palladiumcarbon, ethanol was distilled off under reduced pressure from the filtrate to provide 2.8 g of crude N-(L-prolyl)morpholine (84).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04610821 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-e2675e6625244e5994b3cd4e34c27086 |
| Source note | uspto-grants-1986_09 |