HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vanillin → N-benzyloxycarbony-D-valine isopropylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vanillin | HCID 1183 | — |
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | N-alpha-Benzyloxycarbonyl-D-valine | HCID 712434 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | N-benzyloxycarbony-D-valine isopropylamide | HCID 14723623 | — |
Reaction Steps
Reaction of N-benzyloxycarbonyl-D-valine with isopropylamine by the method of Example 20, Part A afforded a quantitative yield of N-benzyloxycarbonyl-D-valine isopropylamide of Rf 0.61 (TLC, ethyl acetate/hexane, 1:1, vanillin spray).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04411925 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-a78262aeb3914eefbefc37a1791946a5 |
| Source note | uspto-grants-1983_10 |