Acetylacetone → HCID 178454854, compound

HRID 648432Notes

Reaction equation

HRID 648432 reaction equation
[CH2:1]([O:5][Zr:6](OCCCC)([O:12][CH2:13][CH2:14][CH2:15][CH3:16])[O:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH2:2][CH2:3][CH3:4].C(CC(=O)C)(=O)C>C1(C)C=CC=CC=1>[CH2:13]([O:12][Zr:6]([O:7][CH2:8][CH2:9][CH2:10][CH3:11])[O:5][CH2:1][CH2:2][CH2:3][CH3:4])[CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 31261AcetylacetoneHCID 178454855HCID 178454855, compound

Product 1

HCID 178454854HCID 178454854, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

In 88 g of toluene was dissolved 38.3 g (0.1M) of tetra-n-butoxyzirconium, and 10.0 g (0.1M) of acetylacetone was gradually added to the resulting solution with stirring. An exothermic reaction of the mixture took place to give tri-n-butoxyzirconium acetylacetonato.

Workup

  1. additionwas gradually added to the resulting solution
  2. customAn exothermic reaction of the mixture

Sources & evidence

ORD record
ord-79d90e33e52e4a6a810c433e5a6fccf9
Source dataset
uspto-grants-1988_04
Patent number
US04735829

Reaction notes

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