Acetylacetone → HCID 178454853, compound

HRID 648434Notes

Reaction equation

HRID 648434 reaction equation
[CH2:1]([O:5][Zr:6](OCCCC)(OCCCC)[O:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH2:2][CH2:3][CH3:4].C(CC(=O)C)(=O)C>C1(C)C=CC=CC=1>[CH2:8]([O:7][Zr:6][O:5][CH2:1][CH2:2][CH2:3][CH3:4])[CH2:9][CH2:10][CH3:11]

Participants

4

Reactant 2

HCID 31261AcetylacetoneHCID 178454855HCID 178454855, compound

Product 1

HCID 178454853HCID 178454853, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

In 86 g of toluene was dissolved 38.3 g (0.1M) of tetra-n-butoxyzirconium, and 30.0 g (0.3M) of acetylacetone was gradually added to the resulting solution with stirring. An exothermic reaction of the mixture took place to give di-n-butoxyzirconium trisacetylacetonato.

Workup

  1. additionwas gradually added to the resulting solution
  2. customAn exothermic reaction of the mixture

Sources & evidence

ORD record
ord-ae858fa764694db59b55594dfc45b52a
Source dataset
uspto-grants-1988_04
Patent number
US04735829

Reaction notes

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