HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14127357, compound → HCID 14127358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14127357 | HCID 14127357 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14127358 | HCID 14127358 | 86.4% |
Reaction Steps
A mixture of 4.79 g (0.018 mole) of 4-phenYl-1-(phenylmethyl)-3-pyrrolidinemethanamine, 0.7 g of 20% palladium on carbon, and 250 ml of methanol was shaken in an atmosphere of hydrogen at about 50 psi and at room temperature for 24 hours. The catalyst was filtered and the filtrate evaporated under reduced pressure to give 2.74 g of 4-phenyl-3-pyrrolidinemethanamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04735949 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-d2707f1ec68d464a8a46e0323166971a |
| Source note | uspto-grants-1988_04 |