Hydroxylamine → HCID 136332181, compound

Participants

Reaction Steps

A solution of 4-formyl-2-methylamino-5-(4-pyridyl)thiazole (0.9 g) in methanol (15 ml) was added to a 1N-methanolic hydroxylamine solution (5.8 ml) at ambient temperature with stirring, which was continued under the same condition for 2 hours. The precipitate was collected by filtration and recrystallized from an aqueous tetrahydrofuran to afford 4-hydroxyiminomethyl-2-methylamino-5-(4-pyridyl)thiazole (1.02 g).

Provenance & Evidence