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HRID64866

反应详情

EQUATION

反应方程式

HRID 64866 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(C(=O)Cl)cc1
HCID7477

Benzoyl chloride, 4-methoxy-

C8H7ClO2

结构：O=C(CN1CCNCC1)N1CCOCC1
HCID100622

1-(4-Morpholinyl)-2-(1-piperazinyl)ethanone

C10H19N3O2

PRODUCTS

生成物

1
结构：COc1ccc(C(=O)N2CCN(CC(=O)N3CCOCC3)CC2)cc1.Cl
HCID13371227

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

10.25 g of piperazin-1-yl-acetic acid morpholide are cooled to 0° C. in 20 ml of methylene chloride. 8.75 g of anisoyl chloride are added dropwise in the course of 15 minutes. After the mixture has been subsequently stirred for 4 hours, it is diluted with isopropanol, whereupon the colourless product precipitates. It is filtered off with suction and dried.

WORKUP

后处理

  1. customprecipitates
  2. filtrationIt is filtered off with suction
  3. customdried