HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetonitrile → 2-(Hydroxyimino)-2-phenylacetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetonitrile | HCID 8794 | — |
| Reactant | Methyl nitrite | HCID 12231 | — |
| Solvent | HCID 178501943 | HCID 178501943 | — |
| Product | 2-(Hydroxyimino)-2-phenylacetonitrile | HCID 69998 | — |
Reaction Steps
This compound is prepared from benzyl cyanide by reaction with methyl nitrite in CH3OH/CH3ONa in accordance with the method described in Org. Synthesis 59, 95 (1979). Colourless crystals with a melting point of 119°-121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04736055 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-3bb40da495c14013b0f2f7d27360053f |
| Source note | uspto-grants-1988_04 |