HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13477036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 67913319 | HCID 67913319 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13477036 | HCID 13477036 | 105.6% |
Reaction Steps
The methyl 5-bromo-2-naphthylvinyl ether (2.8 g) dissolved in tetrahydrofuran (55 ml) was stirred with concentrated hydrochloric acid (10 ml) for 1 hour at room temperature. Ether and water were added and the organic solution separated and washed with water, saturated sodium bicarbonate and saturated sodium chloride solutions. Evaporation gave a liquid (2.8 g), nD20 =1.6444.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04736065 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-972a31d12e7f47f387ed8bcd26e49785 |
| Source note | uspto-grants-1988_04 |