HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 13654961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 2-Methylthio-1,3-dithiolium perchlorate | HCID 23039009 | — |
| Product | HCID 13654961 | HCID 13654961 | 73.6% |
Reaction Steps
1.0 ml of piperidine and 2.5 g of 2-methylthio-1,3-dithiolium perchlorate were treated in the same manner as in Example 26, and the product was recrystallized from acetone-ethyl ether, whereby 2.1 g (yield: 73.6%) of 1-(1,3-dithiol-2-ylidene)piperidinium perchlorate (Compound No. 34) was obtained as crystals having a melting point of from 171° to 172° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04737494 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-b95e7b752f4c402db3ae2e010c7586cc |
| Source note | uspto-grants-1988_04 |