HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiazoline → HCID 13654964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiazoline | HCID 120269 | — |
| Reactant | 2-Methylthio-1,3-dithiolium perchlorate | HCID 23039009 | — |
| Product | HCID 13654964 | HCID 13654964 | 79.3% |
Reaction Steps
1.0 g of thiazoline and 2.5 g of 2-methylthio-1,3-dithiolium perchlorate were treated in the same manner as in Example 26, and the product was recrystallized from ethanol, whereby 2.3 g (yield: 79.3%) of 3-(1,3-dithiol-2-ylidene)thiazolidinium perchlorate (Compound No. 36) was obtained as crystals having a melting point of from 179° to 180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04737494 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-85a663faa196460ca3aeb22a97086b42 |
| Source note | uspto-grants-1988_04 |