HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 13520695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3,4-Dimethoxy-1,2-benzenediacetonitrile | HCID 10036245 | — |
| Product | HCID 13520695 | HCID 13520695 | — |
Reaction Steps
Here, 3,4-dimethoxy-o-phenylene-diacetonitrile (3.7 g, 0.017 mol) is suspended in glacial acetic acid (10 ml) and mixed with 30% hydrobromic acid (12 ml) in glacial acetic acid at 20° C. The mixture is stirred for 3 hours at ambient temperature, the precipitate is suction filtered, washed with glacial acetic acid and then with acetone/ether and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04737495 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-22eebc8fa42c4ba581bbafe0b9f8a1ea |
| Source note | uspto-grants-1988_04 |