Ammonia → 3-(4-Pyridinylamino)benzamide

HRID 64896Notes

Reaction equation

HRID 64896 reaction equation
[N:1]1[CH:6]=[CH:5][C:4]([NH:7][C:8]2[CH:9]=[C:10]([CH:14]=[CH:15][CH:16]=2)[C:11](O)=[O:12])=[CH:3][CH:2]=1.[NH3:17]>>[N:1]1[CH:6]=[CH:5][C:4]([NH:7][C:8]2[CH:9]=[C:10]([CH:14]=[CH:15][CH:16]=2)[C:11]([NH2:17])=[O:12])=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 222AmmoniaHCID 137124753-[(Pyridin-4-yl)amino]benzoic acid

Product 1

HCID 137124763-(4-Pyridinylamino)benzamideYield 50%

Procedure

3-(4-Pyridinylamino)benzamide was prepared from 3-(4-pyridinylamino)benzoic acid and ammonia according to the procedure of Example 48, part (b), and was obtained in 50% yield as a colorless powder, m.p. 201°-203° C. when recrystallized from methanol.

Workup

  1. customwas obtained in 50% yield as a colorless powder, m.p. 201°-203° C. when
  2. customrecrystallized from methanol

Sources & evidence

ORD record
ord-97b00eea7a994df3861f4e4a6b98738e
Source dataset
uspto-grants-1986_09
Patent number
US04610991

Reaction notes

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