HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 131715490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | t-Boc-Ala-Val-Lys(CBZ)-NH2 | HCID 131715492 | — |
| Product | HCID 131715490 | HCID 131715490 | 83% |
Reaction Steps
The protected tripeptide amide (IX) (1.0 g, 1.8 mmol) was dissolved in cold TFA (10 ml). After 10 minutes, the mixture was evaporated in vacuo and the residue was triturated with ether (2×50 ml). The mother liquors were decanted and the residue was dried under vacuum to give (X) as a foam (0.85 g; 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04737487 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-4c478d8436bf4b2698a8c802e6b06b61 |
| Source note | uspto-grants-1988_04 |