HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenol → HCID 13079890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Reactant | Quinoline, 3-fluoro-4-nitro-, 1-oxide | HCID 87158 | — |
| Reactant | 3-Bromo-7-chloroquinoline | HCID 14555933 | — |
| Product | HCID 13079890 | HCID 13079890 | — |
Reaction Steps
Ethyl 2-{4-[(7-chloroquinolin-3-yl)oxy]phenoxy}propionate (5) was prepared from 3-bromo-7-chloroquinoline, 4-methoxyphenol and ethyl 2-bromopropionate following essentially the same procedure as that described in Example 1 parts (a), (b) and (c). The product, a pale yellow oil, was characterized by its proton magnetic resonance spectrum. Pmr spectrum (CDCl3 ; δ in ppm): 9.75 (1H, d); 8.06 (1H, bs); 7.41 (3H, m); 7.00 (4H, s); 4.75 (1H, q); 4.21 (2H, q); 1.62 (3H, d); 1.27 (3H, t).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04738710 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-5c2d0c0677df4fa9b30332d93ef54e29 |
| Source note | uspto-grants-1988_04 |