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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649142Generated: October 29, 2026

Acetic-formic anhydride → HCID 86742105, compound

https://huagongshe.com/reaction/649142

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic-formic anhydrideHCID 75269—
ReactantSodium bis(2-methoxyethoxy)aluminiumhydrideHCID 21584525—
ReactantHCID 71355693HCID 71355693—
ProductHCID 86742105HCID 86742105—

Reaction Steps

cis-3-Azidomethyl-1-benzyl-4-fluoropyrrolidine was reduced with sodium bis-(2-methoxyethoxy)aluminium hydride and formylated with formic acid-acetic anhydride to yield cis-1-benzyl-4-fluoro-3-formylaminomethylpyrrolidine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04738968
Source datasetuspto-grants-1988_04
ORD IDord-80b4c07f18ed4fc3b77e7a28236d6ebe
Source noteuspto-grants-1988_04