HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanimidic acid, N-cyano-, ethyl ester → HCID 54246393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanimidic acid, N-cyano-, ethyl ester | HCID 9920370 | — |
| Reactant | HCID 20142444 | HCID 20142444 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54246393 | HCID 54246393 | 37.7% |
Reaction Steps
Ethyl N-cyanoformimidate (3.2 g) was added to a suspension of 3-amino-7-chloro-2-ethylimidazo[2,1-a]isoquinoline (2.3 g) in ethanol (60 ml) and the mixture was stirred at room temperature for 45 hours. The mixture was evaporated in vacuo and the residual solid was washed successively with diethyl ether and ethyl acetate to give N-cyano-N'-(7-chloro-2-methylimidazo[2,1-a]isoquinolin-3-yl)formamidine (1.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04738967 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-0d0c8a137f104508b1ecb4eeca710c3f |
| Source note | uspto-grants-1988_04 |