Potassium Hydroxide → HCID 13713130, compound

HRID 64917Notes

Reaction equation

HRID 64917 reaction equation
C([O:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[CH:12]=[C:13]([Cl:15])[Cl:14])(=O)C.[OH-].[K+]>C(O)C>[Cl:14][C:13]([Cl:15])=[CH:12][C:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=1[CH2:5][OH:4]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 13713129HCID 13713129, compound

Product 1

HCID 13713130HCID 13713130, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

133 g (0.54 mole) of 2-(2,2-dichlorovinyl)-benzyl acetate are dissolved in 200 ml of ethanol, and the solution is added, at room temperature, to 750 ml of an ethanolic KOH solution saturated at room temperature. After 2 hours, the mixture is evaporated down, the residue is taken up with H2O, the solution is extracted several times by shaking with ether, and the combined ether phases are washed with H2O, dried and evaporated down.

Workup

  1. customthe mixture is evaporated down
  2. extractionthe solution is extracted several times
  3. washthe combined ether phases are washed with H2O
  4. customdried
  5. customevaporated down

Sources & evidence

ORD record
ord-9ec3a31eca2b4c19829fb4a0dd2ec017
Source dataset
uspto-grants-1986_09
Patent number
US04611010

Reaction notes

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