HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthaloyl chloride → 2-Methoxyanthraquinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthaloyl chloride | HCID 6955 | — |
| Reactant | Anisole | HCID 7519 | — |
| Product | 2-Methoxyanthraquinone | HCID 18646 | 79.8% |
Reaction Steps
The method was similar to that in Example 1, using 10.8 g (0.1 mols) of anisole and 20.2 g (0.1 mols) of phthalic acid dichloride. The product was 19.0 g (60% yield) of 2-methoxy-9,10-anthraquinone (13), m.p. 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04739062 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-198ac111e29e4e98950e400ac618c669 |
| Source note | uspto-grants-1988_04 |