HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → HCID 13823145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | 56541-06-1 | HCID 13823150 | — |
| Product | HCID 13823145 | HCID 13823145 | 65% |
Reaction Steps
The procedure described in Example 1 was repeated, using the N-methyl-4-(3-pyridinyl)-2-thiazolamine prepared in Example 14 and an excess of 1-bromopropane as the reactants. The title compound was purified by column chromatography (65% yield) and converted to its HCl salt by the procedure of Example 2. The resulting salt (mp 138° C.) contained 1.25 molecules of HCl and one molecule of water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04739067 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-4b929f4a59cf49f9a47b9d2e1000e64c |
| Source note | uspto-grants-1988_04 |