HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13823146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Bromopentane | HCID 8057 | — |
| Reactant | 56541-06-1 | HCID 13823150 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13823146 | HCID 13823146 | 53% |
Reaction Steps
The procedure of Example 1 was repeated, using the N-methyl-4-(3-pyridinyl)-2-thiazolamine prepared in Example 14 and an excess of 1-bromopentane as the reactants. The title compound was purified by column chromatography (53% yield) and converted to its HCl salt by the procedure of Example 2. The salt obtained (mp 168°-172° C.) contained 1.5 molecules of HCl and one molecule of water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04739067 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-2b88aa49f14a458aab4e6fc22133e966 |
| Source note | uspto-grants-1988_04 |