HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 1,1-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)-2-ethylhexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-Ethylhexanal | HCID 31241 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Product | 1,1-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)-2-ethylhexane | HCID 13710011 | — |
Reaction Steps
The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 6.41 grams of 2-ethylhexanal, and 150 ml of methyl alcohol. The product is purified by dry-column chromatography to give 10.29 grams of a clear syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04611023 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-6fd87e6b59f448079a43bff64df13065 |
| Source note | uspto-grants-1986_09 |