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HRID649494

反应详情

EQUATION

反应方程式

HRID 649494 的结构方程式

REACTANTS

反应物

2
结构：Cc1nc2cc(Cl)ccc2o1
HCID29510

5-Chloro-2-methylbenzoxazole

C8H6ClNO

结构：CS(=O)(=O)NCCOS(=O)(=O)c1ccc(Cl)cc1
HCID20141389

未命名化合物

PRODUCTS

生成物

1
结构：Cc1oc2ccc(Cl)cc2[n+]1CCNS(C)(=O)=O.O=S(=O)([O-])c1ccc(Cl)cc1
HCID20141390

未命名化合物

PROCEDURE

实验过程

The desired crystal was obtained by carrying out the same synthesis as used in Synthesis Example 1 using 4.2 g (25 mmols) of 5-chloro-2-methylbenzoxazole and 15.7 g (50 mmols) of 2-methanesulfonylaminoethyl-4-chlorobenzenesulfonate. Yield: 7.3 g (60.8%).

WORKUP

后处理

  1. customThe desired crystal was obtained
  2. customthe same synthesis