HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(N-Formyl-L-alpha-aspartyl)-3-phenyl-L-alanine → N-formyl-L-beta-aspartyl-L-phenylalanine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(N-Formyl-L-alpha-aspartyl)-3-phenyl-L-alanine | HCID 92472 | — |
| Reactant | L-phenylalanine sodium salt monohydrate | HCID 70475747 | — |
| Product | N-formyl-L-beta-aspartyl-L-phenylalanine | HCID 13922706 | 30% |
Reaction Steps
Thereafter, the N-formyl-L-α-aspartyl-L-phenylalanine (hereinafter simply referred to as For-α-AP) in the reaction mixture was quantitatively analyzed by HPLC (High performance Liquid Chromatography), to find that it had been formed in a Yield of 68.2% based on the L-phenylalanine sodium salt monohydrate. In addition, 30.0% of N-formyl-L-β-aspartyl-L-phenylalanine (For-β-AP), etc. had been by-produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04740616 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-f6588a4a69ac4866adf842399b69ed7c |
| Source note | uspto-grants-1988_04 |