HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-Chloro-6-(1-methylethyl)benzenamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Chloroaniline | HCID 7240 | — |
| Reactant | Propylene | HCID 8252 | — |
| Product | 2-Chloro-6-(1-methylethyl)benzenamine | HCID 18981698 | — |
Reaction Steps
2-chloro-6-isopropyl aniline was prepared by the method of Example 2 using an H-Y zeolite catalyst for the condensation of aniline and propylene. 2-chloroaniline and propylene were fed to the reactor in a 1:5 mole ratio and LHSV of 0.25 based on 2-chloroaniline. The reaction was conducted at 250° C. and 1343 psig. The effluent product stream was analyzed by gas chromatography. Conversion of 2-chloroaniline was 72%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04740620 |
| Source dataset | uspto-grants-1988_04 |
| ORD ID | ord-b27834cdd4fe414bb73bebecc93a2fb9 |
| Source note | uspto-grants-1988_04 |