HCID 86757231, compound → HCID 22392254, compound

HRID 649714Notes

Reaction equation

HRID 649714 reaction equation
[Cl-:1].C([NH:5][C:6]1[CH:35]=[CH:34][C:33]([NH2:36])=[CH:32][C:7]=1[O:8][CH2:9][CH2:10][CH2:11][N+:12]1[CH:16]=[CH:15][N:14]([CH2:17][CH2:18][CH2:19][O:20][C:21]2[CH:26]=[C:25]([NH2:27])[CH:24]=[CH:23][C:22]=2[NH:28]C(=O)C)[CH:13]=1)(=[O:4])C>O>[OH2:4].[ClH:1].[ClH:1].[ClH:1].[ClH:1].[Cl-:1].[NH2:5][C:6]1[CH:35]=[CH:34][C:33]([NH2:36])=[CH:32][C:7]=1[O:8][CH2:9][CH2:10][CH2:11][N+:12]1[CH:16]=[CH:15][N:14]([CH2:17][CH2:18][CH2:19][O:20][C:21]2[CH:26]=[C:25]([NH2:27])[CH:24]=[CH:23][C:22]=2[NH2:28])[CH:13]=1

Participants

3

Reactant 1

HCID 86757231HCID 86757231, compound

Product 1

HCID 22392254HCID 22392254, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Starting with 23.5 g (0.0454 mol) of 1,3-bis [3-(2-acetylamino-5-aminophenoxy)propyl]-3H-imidazol-1-ium chloride synthesized above in the previous step, 15.0 g of white crystals melting with decomposition at 210-215° C. (Kofler) were obtained, the 1H NMR of which was in accordance and the elemental analysis of which, calculated for C21H33N6O2Cl5.H2O, was:

Workup

  1. custommelting with decomposition at 210-215° C.
  2. customwere obtained

Sources & evidence

ORD record
ord-3cdfe7fd706f482eba91acd301c20a58
Source dataset
uspto-grants-2001_08
Patent number
US06270533B1

Reaction notes

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