Dimethyl Ether → HCID 129652779, compound

Participants

Reaction Conditions

Reaction Steps

First of all, the polysilane to be employed in this example was synthesized as follows. Namely, a mixture comprising 60 mL (milliliter) of dried diethyl ether and 5.34 g of dichlorozirconocene were stirred in an argon atmosphere at a temperature of −20° C., during which 1.6 μm methyl ether was added little by little to the mixture. After continuing the stirring for 70 minutes, the mixture was further stirred at 0° C. for another 30 minutes. Thereafter, diethyl ether was removed and a white solid thus produced was allowed to sublimate to obtain methylzirconocene.

Provenance & Evidence