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HRID649902

反应详情

EQUATION

反应方程式

HRID 649902 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1ccc(F)cc1F
HCID67967

1-Nitro-2,4-difluorobenzene

C6H3F2NO2

结构：CCOC(=O)c1c(N)sc2cc(C)ccc12
HCID18422153

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1c(Nc2cc(F)ccc2[N+](=O)[O-])sc2cc(C)ccc12
HCID18422188

未命名化合物

收率 71.2%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

In the same manner as in Starting Material Synthesis Example 4 and using ethyl 2-amino-6-methylbenzo[b]thiophene-3-carboxylate (4.5 g), 2,4-difluoronitrobenzene (3.1 g) and dimethyl sulfoxide, ethyl 2-(5-fluoro-2-nitroanilino)-6-methylbenzo[b]thiophene-3-carboxyiate (5.1 g) was obtained.

WORKUP

后处理

  1. customMaterial Synthesis Example 4