1-Fluoro-2-nitrobenzene → HCID 18422360, compound

HRID 649947Notes

Reaction equation

HRID 649947 reaction equation
[NH2:1][C:2]1[S:6][C:5]2[C:7]([CH3:11])=[CH:8][CH:9]=[CH:10][C:4]=2[C:3]=1[C:12]#[N:13].F[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[N+:21]([O-:23])=[O:22]>>[CH3:11][C:7]1[C:5]2[S:6][C:2]([NH:1][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[N+:21]([O-:23])=[O:22])=[C:3]([C:12]#[N:13])[C:4]=2[CH:10]=[CH:9][CH:8]=1

Participants

3

Reactant 2

HCID 738951-Fluoro-2-nitrobenzeneHCID 18422198HCID 18422198, compound

Product 1

HCID 18422360HCID 18422360, compound

Procedure

In the same manner as in Starting Material Synthesis Example 51 and using 2-amino-7-methylbenzo[b]thiophene-3-carbonitrile and 2-fluoronitrobenzene, 7-methyl-2-(2-nitroanilino)benzo[b]thiophene-3-carbonitrile is obtained.

Workup

  1. customMaterial Synthesis Example 51

Sources & evidence

ORD record
ord-07f22ec2a954428a98e5464bbd8564db
Source dataset
uspto-grants-2001_08
Patent number
US06271225B1

Reaction notes

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