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HRID649949

反应详情

EQUATION

反应方程式

HRID 649949 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc([N+](=O)[O-])c(F)c1
HCID67966

Benzene, 2-fluoro-4-methyl-1-nitro-

C7H6FNO2

结构：N#Cc1c(N)sc2cc(F)ccc12
HCID18422184

2-Amino-6-fluoro-1-benzothiophene-3-carbonitrile

C9H5FN2S

PRODUCTS

生成物

1
结构：Cc1ccc([N+](=O)[O-])c(Nc2sc3cc(F)ccc3c2C#N)c1
HCID18422235

未命名化合物

收率 88.1%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

In the same manner as in Starting Material Synthesis Example 51 and using 2-amino-6-fluorobenzo[b]thiophene-3-carbonitrile (5.0 g), 3-fluoro-4-nitrotoluene (4.7 g) and dimethyl sulfoxide (55 ml), 6-fluoro-2-(5-methyl-2-nitroanilino)benzo[b]thiophene-3-carbonitrile (7.5 g) was obtained.

WORKUP

后处理

  1. customMaterial Synthesis Example 51