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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 649958Generated: November 1, 2026

1,1-Ethanedithiol → HCID 18422214, compound

https://huagongshe.com/reaction/649958

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1-EthanedithiolHCID 33645—
ReactantAluminum(III) ChlorideHCID 6451240—
ReactantHCID 18422324HCID 18422324—
SolventDichloromethaneHCID 6344—
ProductHCID 18422214HCID 18422214—

Reaction Steps

In the same manner as in Example 62 and using 8-fluoro-4-methoxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine, dichloromethane, ethanedithiol and aluminium chloride, 8-fluoro-4-hydroxy-12-(4-methylpiperazin-1-yl)-6H-[1]benzothieno[2,3-b][1,5]benzodiazepine is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06271225B1
Source datasetuspto-grants-2001_08
ORD IDord-e7f8b6eb36d04a8f97cf474759d8d20c
Source noteuspto-grants-2001_08