HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → N-(2-hydroxy-5-nitrophenyl)-2-bromo-5-methyl-3-thiophenecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Bromo-5-methylthiophene-3-carboxylic acid | HCID 11117589 | — |
| Reactant | 2-Amiino-4-nitrophenol | HCID 86757234 | — |
| Product | N-(2-hydroxy-5-nitrophenyl)-2-bromo-5-methyl-3-thiophenecarboxamide | HCID 18422350 | — |
Reaction Steps
In the same manner as in Starting Material Synthesis Example 67 and using 2-bromo-5-methyl-3-thiophenecarboxylic acid, thionyl chloride and 2-amiino-4-nitrophenol, N-(2-hydroxy-5-nitrophenyl)-2-bromo-5-methyl-3-thiophenecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271225B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-41ccfd4a7df7486884dadee8e93ed816 |
| Source note | uspto-grants-2001_08 |