HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18604483, compound → (+/-)-trans-7-Phenylcarbamoyloxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)quinoline hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18604483 | HCID 18604483 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (+/-)-trans-7-Phenylcarbamoyloxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)quinoline hydrochloride | HCID 18604479 | — |
Reaction Steps
(±)-trans-7-Phenylcarbamoyloxy-4-benzyl-1,2,3,4,4a,5,6,10b-Octahydrobenzo(f)quinoline hydrochloride (40 mg, 0.12 mmol) was dissolved in MeOH (5 ml) and hydrogenolyzed in the presence of 10% Pd/C (40 mg) at 25 psig at room temperature. After filtration of the catalyst and evaporation of the solvent the desired product (20 mg) was obtained. MS shows M+ at m/e 322.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04612316 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-b1c96b76e7954a56823bb853d09e7021 |
| Source note | uspto-grants-1986_09 |