HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl [2-(benzyloxy)ethoxy]acetate → Ethyl (2-hydroxyethoxy)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl [2-(benzyloxy)ethoxy]acetate | HCID 54389372 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl (2-hydroxyethoxy)acetate | HCID 46398405 | 104.1% |
Reaction Steps
A mixture of ethyl (2-benzyloxyethoxy)acetate (0.50 g, 1.88 mmol), 10% palladium-carbon (0.05 g) and methanol (10 ml) was stirred under a hydrogen atmosphere at room temperature for 5 hours. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to obtain 0.29 g of ethyl (2-hydroxyethoxy)acetate as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271251B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-ecf3d72342874ed5aaa0409ec43dedf3 |
| Source note | uspto-grants-2001_08 |