Benzyl isocyanate → HCID 9838850, compound

Participants

Reaction Steps

N-(2-Hydroxy-4-nitrophenyl)-N′-(benzyl)urea was prepared from 2-hydroxy 4-nitro aniline (308 mg, 2.0 mmol) and benzyl isocyanate (2 mmol) according to the procedure in General Method A. The product was purified by dilution with methylene chloride and precipitation with hexanes. Filtering afforded the title compound (362 mg, 52%). EI-MS m/z 288 (M+H)+

Provenance & Evidence