Phenethyl isocyanate → HCID 21714409, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of phenethyl isocyanate (382 mg, 2.6 mmol) in toluene, 2-amino-5-nitrophenol (400 mg, 2.6 mmol) was added. The reaction mixture was stirred at 80° C. for 24 hours, then cooled to room temperature. The product was purified by precipitation from toluene and filtering (650 mg, 83%). m.p: 188.6-189.4° C.; EI-MS m/z 302 (M+H)+.

Provenance & Evidence