Tetrafluoro-m-phenylenediamine dihydrochloride → HCID 86757235, compound

Participants

Reaction Conditions

Reaction Steps

23.22 9 of N,N-diallylpyrrolidinium bromide (EXAMPLE 1) and 3.34 g of diallylarnmonium chloride (EXAMPLE 7) were dissolved in 26.5 g of deionized water to make a 50% solution of the monomer. To the monomer solution was added 1.6 g of 2,2′-azobis(2-am-indinopropane) dihydrochloride and the reaction mixture was bubbled with a slow stream of nitrogen gas for 45 minutes. While stirring the temperature was raised to 70° C. for 48 hours. After cooling to room temperature, 55 g of viscous polymer solution was obtained.

Provenance & Evidence