Water → HCID 86757237, compound

Participants

Reaction Conditions

Reaction Steps

N,N-diallylhomopiperidinium bromide (13.0 g, EXAMPLE 4) and diallylammonium chloride (2.7 g, EXAMPLE 7) were dissolved in 15.0 g deionized water. To this aqueous solution was added 0.5 g of 2,2′-azobis(2-amidinopropane) dihydrochloride, the reaction mixture was bubbled with a slow stream of nitrogen gas for 45 minutes. While stirring, the temperature was raised to 70° C. The reaction mixture was stirred at 70° C. for 48 hours. After cooling to room temperature, 30.0 g of viscous polymer solution was obtained.

Provenance & Evidence