Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(+-)-1-Aminoindan → HCID 18627820, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (+-)-1-Aminoindan | HCID 123445 | — |
| 반응물 | 4-(Dipropylsulfamoyl)benzoyl chloride | HCID 2735528 | — |
| 생성물 | HCID 18627820 | HCID 18627820 | 63% |
반응 단계
The title compound was prepared in 63% yield from (rac)-1-aminoindan (10.0 g, 75.2 mmole) and 4-(di-n-propylsulfamoyl) benzoyl chloride (16.3 g, 53.6 mmole, prepared from probenecid and SOCl2) via a procedure analogous to that described in Ex. 46, followed by crystallization from hexane:EtOAc, mp: 124-5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06271263B1 |
| 출처 데이터셋 | uspto-grants-2001_08 |
| ORD ID | ord-71292d2893d94fee95049bb29f3de9eb |
| 출처 메모 | uspto-grants-2001_08 |