Cyclohexanone → HCID 13352199, compound

HRID 65017Notes

Reaction equation

HRID 65017 reaction equation
[C:1]1([N:7]2[C:11]([NH2:12])=[CH:10][C:9]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:19]1(=O)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>>[C:1]1([N:7]2[C:11]([NH2:12])=[C:10]([C:19]3[CH2:24][CH2:23][CH2:22][CH2:21][CH:20]=3)[C:9]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)=[N:8]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 7967CyclohexanoneHCID 1999691,3-Diphenyl-1H-pyrazol-5-amine

Product 1

HCID 13352199HCID 13352199, compound

Procedure

It is obtained by essentially following the procedure of example 1, reacting 1,3-diphenyl-5-pyrazolamine (1 mole) with cyclohexanone (1.1 mole) at a temperature of about 80° C. for about 4 hours. M.p. 115°-117° C.

Workup

  1. customIt is obtained
  2. customat a temperature of about 80° C.
  3. customfor about 4 hours

Sources & evidence

ORD record
ord-2cf524c864a4495a972218d489695bf3
Source dataset
uspto-grants-1986_09
Patent number
US04612318

Reaction notes

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