HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 53706054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | (1R,2R)-2-Aminocyclohexanol | HCID 735777 | — |
| Product | HCID 53706054 | HCID 53706054 | — |
Reaction Steps
Trans-2-amino-cyclohexanol (Aldrich) is treated with triphosgene in methylene chloride (1/3 equivalent). To the resulting solution, excess ammonium hydroxide is added to give after work up the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271358B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-db405dd2a5f3414e9cf05d20d9832df3 |
| Source note | uspto-grants-2001_08 |