Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Lilial → HCID 11012960, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Lilial | HCID 228987 | — |
| 반응물 | Sodium cyanoborohydride | HCID 5003444 | — |
| 반응물 | 5-(Aminomethyl)-2-chloropyridine | HCID 7020927 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 11012960 | HCID 11012960 | — |
반응 단계
Route A: After suspending 620 mg (9.84 mmol) of sodium cyanoborohydride in 2 ml of absolute methanol, 700 mg (4.91 mmol) of 6-chloro-3-pyridylmethylamine was added thereto. Subsequently, to this was added a solution of 1.0 g (4.90 mmol) 3-(4-t-butylphenyl)-2-methylpropionaldehyde/2 ml absolute methanol by portions and then, stirring was conducted at room temperature for 4 h.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06271385B1 |
| 출처 데이터셋 | uspto-grants-2001_08 |
| ORD ID | ord-6b8c0a22c7ca4e8ea28cefd9cd3dcabd |
| 출처 메모 | uspto-grants-2001_08 |