HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → Isoamyl Cyanoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Isoamyl Alcohol | HCID 31260 | — |
| Reactant | Cyanoacetate | HCID 1551036 | — |
| Product | Isoamyl Cyanoacetate | HCID 21714940 | — |
Reaction Steps
Using the procedure of Example 1, cyanoacetate acid (85.5 g; 1.00 mol) and isoamyl alcohol (176 g; 2 mol) are reacted in the presence of sulfuric acid (0.49 g; 0.005 mol). Isoamyl cyanoacetate (bp 133/20 mm of Hg) is recovered as a clear liquid. The yield was 150 g (97% of theoretical) and its purity was >99% (GC assay).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271410B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-85d371c307e6489fbdbfd936ddb8c73c |
| Source note | uspto-grants-2001_08 |