Indene → HCID 15534874, compound

Participants

Reaction Steps

20 ml of triethylamine, 2.2 g (20 mmole) of indene, 4.77 g (20 mmole) of para-chloro iodo-benzene and 0.134 g (0.6 mmole) of Pd(OAc)2 were stirred under reflux for 10 h. After that the mixture was cooled to room temperature and treated with 100 ml of ethanol. The crystalline precipitate was isolated, washed with cold ethanol and dried under vacuum to obtain 2.53 g (56%) of 2-(4-chloro-phenyl)-indene.

Provenance & Evidence