HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodonaphthalene → HCID 18413732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodonaphthalene | HCID 7004 | — |
| Reactant | Indene | HCID 7219 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Product | HCID 18413732 | HCID 18413732 | 31% |
Reaction Steps
20 ml of triethylarine, 2.2 g (20 mmole) of indene, 5.08 g (20 mmole) of 1-naphtyl-iodide and 0.134 g (0.6 mmole) of Pd(OAc)2 were stirred under reflux for 10 h. After that the mixture was cooled to room temperature and evaporated. The residual oil was recrystallized from ethanol and dried under vacuum to obtain 1.5 g (31%) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06271411B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-badf71f341064d25b680ea02cefcd71f |
| Source note | uspto-grants-2001_08 |